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KMID : 0903519890320040350
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Journal of the Korean Society of Agricultural Chemistry and Biotechnology
1989 Volume.32 No. 4 p.350 ~ p.356
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Determination of Lignan Compounds in Fruits of Schisandra chinensis BAILLON by Capillary - GC(FID)
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김용하/Kim, Yong Ha
손현주/복진영/백순옥/Sohn, Hyun Joo/Bock, Jin Young/Baik, Soon Ok
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Abstract
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The determinabilities of several lignan compounds by capillary-GC (F1D) were studied. The lignan compounds used were deoxyschizandrin, gomisin N, schizandrin, wuweizisu C, gomisin A, angeloylgomisin H and tigloylgomisin H which were isolated from fruits of Schisandra chinensis BAILLON and identified with GC/MS(EI, 70eV), 1H-NMR(300MHz) and IR. The GC column used was SPB-1 fused silica capillary(0.25㎜ ID×30m, Supelco), and the column oven temperature was programmed from 200℃ to 300℃ at the rate of 4℃ per minute. The linearities between concentration and FID response were maintained in 2∼500ppm of deoxyschizandrin and wuweizisu C and in 5∼500ppm of gomisin N, schizandrin, gomisin A, angeloylgomisin H and tigloylgomisin H. The contents of lignan compounds in fruits of S. chinensis BAILLON Produced at Moo-ju area were analyzed by the GC method: the values obtained of schizandrin and gomisin N were 6.5 and 5.9㎎/g respectively, and those of gomisin A, wuweizisu C, angeloylgomisin H, deoxyschizandrin and tigloylgomisin H were 0.5∼1.6㎎/g.
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KEYWORD
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